Εγκαταστάθηκαν τον Ιούλιο του 2007 Χρηματοδότηση: ΠΡΟΓΡΑΜΜΑ ΑΝΤΑΓΩΝΙΣΤΙΚΟΤΗΤΑΣ, Μέτρο 4.5, Δράση 4.4.1-Πράξη με τίτλο: ΥΠΟΔΟΜΕΣ ΥΠΟΣΤΗΡΙΞΗΣ ΤΗΣ ΜΑΚΡΟΠΡΟΘΕΣΜΗΣ ΒΙΩΣΙΜΟΤΗΤΑΣ ΤΩΝ ΕΡΓΩΝ ΕΡΕΥΝΑΣ, ΤΕΧΝΟΛΟΓΙΚΗΣ ΑΝΑΔΕΙΞΗΣ ΚΑΙ ΕΠΙΔΕΙΞΗΣ. ΤΙΤΛΟΣ ΕΡΓΟΥ: ΣΧΕΔΙΑΣΜΟΣ ΚΑΙ ΣΥΝΘΕΣΗ ΒΙΟΔΡΑΣΤΙΚΩΝ ΜΟΡΙΩΝ
Varian V600 MHz
Αναβαθμίστηκε τον Οκτώβριο του 2010 with 3rd channel accessory and 1H/13C/15N triple resonance probe FP7-REGPOT-2009-1
Features: Magnet: 14.1 Tesla 54 mm bore Varian Superconducting Magnet
Console:
DIRECTDRIVE ARCHITECTURE INCLUDING POWER PC AND XILINX FPGA. Provides total pulse programming control and delivers precisely timed RF events. Complete waveform shaping capability.
3 RF Channels
Channel 1 is highband, with 1H/19F observe, spinlock and decouple capability (550-600 MHz, 50W)
Channels 2 & 3 have broadband observe, spinlock and decouple capability (18-245 MHz, 300 W)
• Performa IV Pulsed Field Gradient Module
• Protune Accessory
• Variable Temperature unit (-150C to +250C, with 0.1C resolution)
Applications
• Single or double resonance studies to fully characterize organic compounds
• DOSY pulse sequence for the separation of mixture components
• Triple resonance experiments of chemical or biomolecular samples. Capability for 1H observation with simultaneous or single irradiation of 13C and 15N frequencies.
Varian V300 MHz
Features: Magnet: 7 Tesla 52 mm bore Oxford Magnet
Console:
DIRECTDRIVE ARCHITECTURE INCLUDING POWER PC AND XILINX FPGA. Provides total pulse programming control and delivers precisely timed RF events. Complete waveform shaping capability.
2 RF Channels
Channel 1 is highband, with 1H/19F observe, spinlock and decouple capability (200-300 MHz, 50W)
Channels 2 has broadband observe, spinlock and decouple capability (12-220 MHz, 300 W and 220-245 MHz, 150 W)
• Performa I Pulsed Field Gradient Module
• Carousel autosampler for 9 samples
• Variable Temperature unit (-15oC to +25oC, with 0.1oC resolution)
Probes: 1 H/19F/31P/13C 5mm PFG AutoSwitchable Host computer: Dell 380N PC, Red Hat Linux Software: VNMRJ 2.2C
Applications
• Single or double resonance studies to fully characterize organic compounds
Varian V400 MHz Solid state
Features: Magnet: 9.4 Tesla WB 89 mm bore Oxford Magnet
Console:
DIRECTDRIVE ARCHITECTURE INCLUDING POWER PC AND XILINX FPGA. Provides total pulse programming control and delivers precisely timed RF events. Complete waveform shaping capability.
2 RF Channels
Channel 1 is highband, with 1H/19F observe, spinlock and decouple capability (400 MHz, 1 KW)
Includes X-HP Solids Single Cabinet
Channels 2 has broadband observe, spinlock and decouple capability (12-220 MHz, 1 KW and 220-240 MHz, 850 W)
• Performa I Pulsed Field Gradient Module
• Variable Temperature unit (-50oC to +100oC, with 0.1oC resolution)
Mass speed controller
Probes: 3.2 mm Double Resonance HX-Mas Solids probe
25 KHz MAS spinning, 31P to 15N observe channel 19F-1H Decouple channel, 147 KHz decoupling strength
Host computer: Dell 380N PC, Red Hat Linux Software: VNMRJ 2.2C
Applications
13C, 31P MAS and CP-MAS with HP 1H decoupling
Drug-membrane interactions
Determination of coordination states of 27Al, 29Si
Drug polymorphism studies
Characterization of other metal complexes
Αποστολή Δειγμάτων
Τα δείγματα θα αποστέλλονται στη διεύθυνση:
Μονάδα Φασματοσκοπίας NMR
Ινστιτούτο Βιολογίας, Φαρμακευτικής Χημείας και Βιοτεχνολογίας
Τμήμα Οργανικής και Φαρμακευτικής Χημείας
ΕΘΝΙΚΟ ΙΔΡΥΜΑ ΕΡΕΥΝΩΝ, Βασ. Κωνσταντίνου 48,
11635, ΑΘΗΝΑ - ΕΛΛΑΔΑ
Τηλ. +30210.72.73.870
Φαξ. +30210.72.73.872
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